2-苯基-1,3-二噻烷合成路线 （共 88 条）
参考文献
Journal of the American Chemical Society, , vol. 74, p. 2962
反应条件
in THF-d8 (tetrahydrofuran-d8) T=-78°C; Inert atmosphereSchlenk technique;
参考文献
Organic Letters, , vol. 16, # 1 p. 70 - 73
反应条件
acetyl chloride 2 h; Heating;
参考文献
Synthetic Communications, , vol. 34, # 24 p. 4545 - 4556
反应条件
in diethyl ether 0.0833333 h; Heating;
参考文献
Synthetic Communications, , vol. 20, # 16 p. 2387 - 2400
反应条件
1: 96 percent / solid silica chloride / acetonitrile / 20 °C 2: 94 percent / solid silica chloride / CHCl3 / 0.33 h / 20 °C View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 177, # 12 p. 2847 - 2858
反应条件
1: 95 percent / solid silica chloride / acetonitrile / 20 °C 2: 94 percent / solid silica chloride / CHCl3 / 0.33 h / 20 °C View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 177, # 12 p. 2847 - 2858
反应条件
1: 79 percent / solid silica chloride / acetonitrile / 20 °C 2: 94 percent / solid silica chloride / CHCl3 / 0.33 h / 20 °C View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 177, # 12 p. 2847 - 2858
反应条件
1: 80 percent / (BzNMe3)Cl / CHCl3; H2O / Ambient temperature 2: 13 percent / 0.2M (NEt4)Br / methanol / electroreduction View Scheme
参考文献
Chemische Berichte, , vol. 121, p. 2245 - 2250
反应条件
tetraethylammonium bromide in methanol electroreduction; Yields of byproduct given;
参考文献
Chemische Berichte, , vol. 121, p. 2245 - 2250
反应条件
boron trifluoride diethyl etherate; NAF 1) CH2Cl2, 0 deg C; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 27, # 52 p. 6305 - 6306
