1,2-乙二醇单乙酸酯合成路线 (共 112 条)
反应条件
T=180°C; P=14710.2 Torr;
参考文献
US1976677 , ;
FR697786 ;
DE595174 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 19, p. 210
反应条件
Pd(MeCN)2Cl(NO2) T=25°C; P=2068.6 Torr; 4 h; various catalysts, times, additives, O2 atmosphere, with 18O containing complex; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 107, # 12 p. 3545 - 3552
反应条件
HY-Zeolite 3.5 h; Heating;
参考文献
Srinivas; Mahender; Das, Biswanath
Synlett, 2003 , # 15 p. 2419 - 2421
反应条件
T=130°C; 3 h; Product distribution / selectivity;
参考文献
LEK PHARMACEUTICALS D.D.; UDOVIC, Marko; TRAMSEK, Marko; PLANTAN, Ivan; CLUZEAU, Jerome
Patent: WO2011/64249 A1, 2011 ;
Location in patent: Page/Page column 23 ;
反应条件
water; acetic acid in hexane Ambient temperature; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 60, # 17 p. 5729 - 5731
反应条件
water; toluene-4-sulfonic acid in dichloromethane 0.5 h; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 61, # 13 p. 4469 - 4471
反应条件
sodium hydride in tetrahydrofuran T=25°C; 24 h;
参考文献
JAOCS, Journal of the American Oil Chemists' Society, , vol. 83, # 3 p. 201 - 207
反应条件
4 A molecular sieve; silver carbonate in dichloromethane Title compound not separated from byproducts;
参考文献
Aitken, David J.; Rees, Lilias; Suckling, Colin J.; Wood, Hamish C. S.
Tetrahedron Letters, 1986 , vol. 27, # 29 p. 3417 - 3420
反应条件
4 A molecular sieve; silver carbonate in dichloromethane Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 27, # 29 p. 3417 - 3420
反应条件
4 A molecular sieve; silver carbonate in dichloromethane Title compound not separated from byproducts;
参考文献
Aitken, David J.; Rees, Lilias; Suckling, Colin J.; Wood, Hamish C. S.
Tetrahedron Letters, 1986 , vol. 27, # 29 p. 3417 - 3420