反应条件
1: 0.5 g / 0.5 h / 260 - 280 °C
2: 83 percent / 10percent Pd/C / various solvent(s) / 8 h / 190 °C
3: 1.) Na, NH3 liq., 2.) AcOH / 1.) THF, 18 h, 2.) 100 deg C to 125 deg C, 18 h
4: 1.) t-BuONa, 2.) DDQ / 1.) t-BuOH, reflux, 15 h, 2.) dioxane, reflux, 15 h
5: 29 mg / I2 / benzene / 12 h / Heating
6: 5percent aq. NaOH / tetrahydrofuran; methanol / 8 h / Ambient temperature
7: pyridine
8: 1.) AIBN, dibromantin, 2.) Li2CO3, LiF / 1.) CCl4, reflux, 30 min, 2.) HMPA, 100 deg C, 3 h
9: 76 percent / NH3 / methanol; tetrahydrofuran / 1.5 h
View Scheme
参考文献
Rosario, Christopher A.; Holder, Gerald M.; Duke, Colin C.
Journal of Organic Chemistry, 1987 , vol. 52, # 6 p. 1064 - 1072
