1,2,3,3-四甲基-3H-吲哚鎓碘化物合成路线 （共 49 条）
反应条件
in nitromethane T=20°C; 12 h;
参考文献
Kiyose, Kazuki; Hanaoka, Kenjiro; Oushiki, Daihi; Nakamura, Tomomi; Kajimura, Mayumi; Suematsu, Makoto; Nishimatsu, Hiroaki; Yamane, Takehiro; Terai, Takuya; Hirata, Yasunobu; Nagano, Tetsuo
Journal of the American Chemical Society, 2010 , vol. 132, # 45 p. 15846 - 15848
反应条件
1: N-methylaniline With acetic acid; sodium nitrite in water T=20°C; 0.75 h; 2: 3-methyl-butan-2-one With acetic acid; zinc Fischer indolization; 0.5 h; Heating; 3: With hydrogen iodide in ethanol
参考文献
Zimmermann, Thomas; Brede, Ortwin
Journal of Heterocyclic Chemistry, 2004 , vol. 41, # 1 p. 103 - 108
反应条件
1: acetic acid / 12 h / |Reflux; |Inert atmosphere 2: acetonitrile / 12 h / |Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 24 p. 7667 - 7671
反应条件
in 1,4-dioxane T=95 - 100°C; 5 h;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 25, # 1 p. 47 - 50
Khimiya Geterotsiklicheskikh Soedinenii, , # 1 p. 57 - 59
反应条件
ethanol; hydrogen iodide T=20°C;
参考文献
Chemische Berichte, , vol. 31, p. 1948
Monatshefte fuer Chemie, , vol. 21, p. 165,167
反应条件
1: acetic acid / 12 h / |Reflux; |Inert atmosphere 2: acetonitrile / 12 h / |Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 24 p. 7667 - 7671
反应条件
in tetrahydrofuran T=70°C; 480 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 121, p. 1009 - 1012
反应条件
in tetrahydrofuran T=22°C; 504 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemische Berichte, , vol. 121, p. 1009 - 1012
反应条件
diethyl ether; hydrogen iodide
参考文献
Chemische Berichte, , vol. 31, p. 613
反应条件
1: diethyl ether 2: aqueous hydrochloric acid 3: Erw. des Rktprod. mit Methanol View Scheme
参考文献
Annales de Chimie (Cachan, France), , vol. <11>17, p. 5,15
