苯基trans-苯乙烯基砜合成路线 （共 15 条）
反应条件
didodecanoyl peroxide in chlorobenzene T=110°C;
参考文献
Angewandte Chemie - International Edition, , vol. 41, # 17 p. 3265 - 3267
反应条件
sodium in various solvent(s) T=254°C; 6 h; var. temp. and time; Product distribution;
参考文献
Tetrahedron Letters, , vol. 39, # 18 p. 2671 - 2674
反应条件
Fe(F20TPP)Cl; dihydrogen peroxide in ethanol
T=20°C; 0.25 h;
参考文献
Baciocchi, Enrico; Gerini, Maria Francesca; Lapi, Andrea
Journal of Organic Chemistry, 2004 , vol. 69, # 10 p. 3586 - 3589
反应条件
n-butyllithium in tetrahydrofuran
参考文献
Ager, David J.
Journal of the Chemical Society, Chemical Communications, 1984 , # 8 p. 486 - 488
反应条件
water; lithium bromide
T=80 - 90°C; 10 h; regioselective reaction;
参考文献
Chawla, Ruchi; Kapoor, Ritu; Singh, Atul K.; Yadav, Lal Dhar S.
Green Chemistry, 2012 , vol. 14, # 5 p. 1308 - 1313
反应条件
ammonium hydroxide in 1,4-dioxane
Ambient temperatureovernight; Yield given;
参考文献
Naidan, V. M.; Naidan, G. D.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 11 p. 2611 - 2615,2117 - 2120
反应条件
1: 1)30percent H2SO4, NaNO2; 2) SO2, copper bromide, KBr / 1) glacial acetic acid; 2) acetic acid-acetone
2: NH4OH / dioxane / Ambient temperature; overnight
View Scheme
参考文献
Naidan, V. M.; Naidan, G. D.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 11 p. 2611 - 2615,2117 - 2120
反应条件
1: 1)30percent H2SO4, NaNO2; 2) SO2, copper bromide, KBr / 1) glacial acetic acid; 2) acetic acid-acetone
2: NH4OH / dioxane / Ambient temperature; overnight
View Scheme
参考文献
Naidan, V. M.; Naidan, G. D.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 11 p. 2611 - 2615,2117 - 2120
反应条件
triethylamine in ethanol
T=25°C; Rate constant;
参考文献
Barlow,K.N. et al.
Journal of the Chemical Society, Chemical Communications, 1973 , p. 175 - 176
反应条件
triethylamine in ethanol
T=25°C; Rate constant;
参考文献
Barlow,K.N. et al.
Journal of the Chemical Society, Chemical Communications, 1973 , p. 175 - 176
