dilithium tetrachlorocuprate; ethylmagnesium bromide 1.) THF, Et2O, from -20 to -10 deg C, 2.) a) -20 deg C, 2 h, b) 25 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mirviss, Stanley B.
Journal of Organic Chemistry, 1989 , vol. 54, # 8 p. 1948 - 1951
gold(III) chloride; N,N,N',N,-tetramethylethylenediamine; copper diacetate; zinc in water T=20°C; 24 h; Inert atmosphere;
参考文献
Lipshutz, Bruce H.; Huang, Shenlin; Leong, Wendy Wen Yi; Zhong, Guofu; Isley, Nicholas A.
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 19985 - 19988
