2-(4-吡啶)-2-噁唑啉合成路线 (共 5 条)
反应条件
bismuth trifluoromethanesulphonate
1.25 h; Heating;
参考文献
Hojati, Seyedeh Fatemeh; Nezhadhoseiny, Seyede Atefe
Journal of the Serbian Chemical Society, 2012 , vol. 77, # 9 p. 1181 - 1189,9
反应条件
sodium hydride in ethylene glycol dimethyl ether
T=20 - 40°C; 29 h;
参考文献
Ikeda, Katsuya; Honda, Hiroyuki; Matsuo, Takanori; Yamamoto, Tamotsu
Organic Preparations and Procedures International, 1995 , vol. 27, # 1 p. 103 - 106
反应条件
2,2'-azo-bisisobutyronitrile; 2-Propenoic acid tert-butyl ester; tri-n-butyl-tin hydride in benzene
T=80°C; 23 h; Inert atmosphere;
参考文献
Wood, Mark E.; Bissiriou, Sabine; Lowe, Christopher; Norrish, Andrew M.; Senechal, Katell; Windeatt, Kim M.; Coles, Simon J.; Hursthouse, Michael B.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 20 p. 4653 - 4665
反应条件
copper(I) bromide dimethylsulfide complex; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
24 h; Heating;
参考文献
Leconte, Nicolas; Pellegatti, Laurent; Tatibouet, Arnaud; Suzenet, Franck; Rollin, Patrick; Guillaumet, Gerald
Synthesis, 2007 , # 6 p. 857 - 864
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene
T=80°C; 18 h; Inert atmosphere;
参考文献
Wood, Mark E.; Bissiriou, Sabine; Lowe, Christopher; Norrish, Andrew M.; Senechal, Katell; Windeatt, Kim M.; Coles, Simon J.; Hursthouse, Michael B.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 20 p. 4653 - 4665