N-(4-乙酰基苯基)苯甲酰胺合成路线 （共 13 条）
反应条件
lithium perchlorate; gallium trifluoromethanesulfonate in nitromethane
T=50°C; Friedel-Crafts acylation; 24 h;
参考文献
Japan Science and Technology Corporation
Patent: EP1359141 A1, 2003 ;
Location in patent: Page/Page column 6-7 ;
反应条件
lithium perchlorate; trifluoroacetic anhydride; gallium trifluoromethanesulfonate in nitromethane
T=50°C; Friedel-Crafts acylation; 24 h;
参考文献
Japan Science and Technology Corporation
Patent: EP1359141 A1, 2003 ;
Location in patent: Page/Page column 6-7 ;
反应条件
triethylamine in tetrachloromethane
2 h; Reflux;
参考文献
Yadlapalli, Rama Krishna; Chourasia; Jogi, Madhu Prakash; Podile, Appa Rao; Perali, Ramu Sridhar
Medicinal Chemistry Research, 2013 , vol. 22, # 6 p. 2975 - 2983
反应条件
CuSO4‵5H2O; potassium carbonate; N-methyl-2-(methylamino)ethylamine in o-xylene
T=130°C; 12 h; regioselective reaction;
参考文献
Panda, Niranjan; Mothkuri, Raghavender; Nayak, Dinesh Kumar
European Journal of Organic Chemistry, 2014 , vol. 2014, # 8 p. 1602 - 1605
反应条件
carbon monoxide; benzene; dodecacarbonyltetrarhodium(0)
T=220°C; 6 h;
参考文献
Mise, Takaya; Hong, Pangbu; Yamazaki, Hiroshi
Chemistry Letters, 1980 , p. 439 - 440
反应条件
in dimethyl sulfoxide; ethyl acetate
T=5 - 20°C; 1 h;
参考文献
Wu, Xinghua; Hu, Longqin
Tetrahedron Letters, 2005 , vol. 46, # 48 p. 8401 - 8405
反应条件
caesium carbonate; bis[hydrotris(3-Me-imidazolin-2-ylidene)borate]triCu(I) BF4 in dimethyl sulfoxide
T=100°C; 24 h;
参考文献
Tubaro, Cristina; Biffis, Andrea; Scattolin, Elena; Basato, Marino
Tetrahedron, 2008 , vol. 64, # 19 p. 4187 - 4195
反应条件
caesium carbonate; bis[hydrotris(3-Me-imidazolin-2-ylidene)borate]triCu(I) BF4 in dimethyl sulfoxide
T=100°C; 24 h;
参考文献
Tubaro, Cristina; Biffis, Andrea; Scattolin, Elena; Basato, Marino
Tetrahedron, 2008 , vol. 64, # 19 p. 4187 - 4195
反应条件
caesium carbonate; bis[hydrotris(3-Me-imidazolin-2-ylidene)borate]triCu(I) BF4 in dimethyl sulfoxide
T=100°C; 24 h;
参考文献
Tubaro, Cristina; Biffis, Andrea; Scattolin, Elena; Basato, Marino
Tetrahedron, 2008 , vol. 64, # 19 p. 4187 - 4195
反应条件
2,6-dimethylpyridine in chloroform
T=30°C; Kinetics;
参考文献
Kolakowski, Robert V.; Shangguan, Ning; Sauers, Ronald R.; Williams, Lawrence J.
Journal of the American Chemical Society, 2006 , vol. 128, # 17 p. 5695 - 5702
