4-羟基-2(5H)-呋喃酮合成路线 (共 17 条)
反应条件
hydrogenchloride; barium dihydroxide; hydrogen; palladium on activated charcoal P=2585.7 Torr; 2.) overnight, 3.) 4 deg C;
参考文献
Schmidt, Diane Grob; Zimmer, Hans
Synthetic Communications, 1981 , vol. 11, # 5 p. 385 - 390
参考文献
Sato; Sakaki; Takayama; Kobayashi; Suzuki; Kaneko
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 1 p. 94 - 98
反应条件
hydrogenchloride T=15 - 20°C; 41 h; Yield given;
参考文献
Heterocycles, , vol. 24, # 5 p. 1429 - 1431
反应条件
trimethylsilyl iodide; water 1) CHCl3, 2 weeks, room temperature; Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 16 p. 1831 - 1834
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane Ambient temperature;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 34, # 12 p. 5188 - 5191
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine; dicyclohexyl-carbodiimide in dichloromethane 15 h; Ambient temperature;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 34, # 12 p. 5188 - 5191
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; p-toluenesulfonyl chloride in tetrahydrofuran; water T=60°C;
参考文献
Hu, Yi; Ding, Qiuping; Ye, Shengqing; Peng, Yiyuan; Wu, Jie
Tetrahedron, 2011 , vol. 67, # 38 p. 7258 - 7262
反应条件
N-bromosuccinmide in ethanol 0.166667 h; Ambient temperature; Yield given;
参考文献
Ge, Ping; Kirk, Kenneth L.
Journal of Fluorine Chemistry, 1997 , vol. 84, # 1 p. 45 - 47
反应条件
in acetic acid T=115 - 120°C; 5 h;
参考文献
Momose, Takefumi; Toyooka, Naoki; Nishi, Takafumi; Takeuchi, Yumi
Heterocycles, 1988 , vol. 27, # 8 p. 1907 - 1924
反应条件
acetyl chloride 4 h; Heating;
参考文献
Gelin, Suzanne; Pollet, Patrick
Synthetic Communications, 1980 , vol. 10, # 11 p. 805 - 812