1-氨基-3-甲基丁烷 盐酸盐合成路线 （共 8 条）
参考文献
LG Chemical Ltd.
Patent: US6268363 B1, 2001 ;
反应条件
ammonium formate; palladium on activated charcoal in methanol
Ambient temperature;
参考文献
Ram, Siya; Ehrenkaufer, Richard E.
Tetrahedron Letters, 1984 , vol. 25, # 32 p. 3415 - 3418
反应条件
1: With tri-ruthenium(0)dodecacarbonyl; (HSiMe2)2NH in toluene
T=20 - 70°C; 24.17 h; Inert atmosphere;
2: With hydrogenchloride in 1,4-dioxane; ethyl acetate; toluene
T=20°C; 0.5 h;
参考文献
Reeves, Jonathan T.; Tan, Zhulin; Marsini, Maurice A.; Han, Zhengxu S.; Xu, Yibo; Reeves, Diana C.; Lee, Heewon; Lu, Bruce Z.; Senanayake, Chris H.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 1 p. 47 - 52
反应条件
hydrogenchloride in diethyl ether
6 h;
参考文献
Sampson, Peter B.; Honek, John F.
Organic Letters, 1999 , vol. 1, # 9 p. 1395 - 1397
反应条件
1: 2,3-dichloro-5,6-dicyanobenzoquinone; molecular sieves 4 Angstroem / benzene / 1 h / 60 °C
2: aq. HCl / diethyl ether / 6 h
View Scheme
参考文献
Sampson, Peter B.; Honek, John F.
Organic Letters, 1999 , vol. 1, # 9 p. 1395 - 1397
反应条件
1: 3-methyl-1-butamine With hydrogenchloride in diethyl ether
2: p-styrenesulfonic acid sodium salt in methanol
T=20°C; 18 h; Further stages. Title compound not separated from byproducts.;
参考文献
Motherwell, William B.; Bingham, Matilda J.; Pothier, Julien; Six, Yvan
Tetrahedron, 2004 , vol. 60, # 14 p. 3231 - 3241
反应条件
1: water; NaOCl / 0 °C
2: petroleum ether
View Scheme
参考文献
Coleman; Andersen; Hermanson
Journal of the American Chemical Society, 1934 , vol. 56, p. 1381
反应条件
1: NaHSO3; water
2: sodium; butanol; toluene
View Scheme
参考文献
Bloom; Breslow; Hauser
Journal of the American Chemical Society, 1945 , vol. 67, p. 539
