2-氨基-3,5-二溴-4,6-二甲基吡啶合成路线 (共 2 条)
反应条件
1: With bromine; acetic acid
T=20°C; 1.25 h; Inert atmosphere;
2: With sodium hydroxide
Inert atmosphereCooling with ice;
参考文献
Zhang, Feng; Zaidi, Saheem; Haney, Kendra M.; Kellogg, Glen E.; Zhang, Yan
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7945 - 7952
反应条件
1: With tert.-butylnitrite; bromine in tribromo methane
T=20°C; Sandmeyer type reaction; 2 h;
2: With sodium carbonate in tribromo methane
参考文献
Zhang, Feng; Zaidi, Saheem; Haney, Kendra M.; Kellogg, Glen E.; Zhang, Yan
Journal of Organic Chemistry, 2011 , vol. 76, # 19 p. 7945 - 7952