反应条件
H2 in perdeuterocyclohexane byproducts: methane; under N2; in a NMR tube Zr complex was dissolved in cyclohexane-d12, thetube was freeze-pump-thaw degassed 3 times, CHF2Cl was condensed at -19 6°C , H2 was added, upon thawing, a yellow ppt. formed, the mixt.was heated at 120°C for 10 d; not isolated, monitored by NMR;
参考文献
Journal of the American Chemical Society, , vol. 123, # 44 p. 10973 - 10979
