二苯基(异硫氰酸基)磷酸酯合成路线 (共 10 条)
参考文献
Bernat, Juraj; Petercakova, Dana; Imrich, Jan; Kutschy, Peter; Kniezo, Ladislav
Zeitschrift fuer Chemie (Stuttgart, Germany), 1988 , vol. 28, # 4 p. 141 - 142
反应条件
in hexane 15 h; Yield given;
参考文献
Bernat, Juraj; Kristian, Pavol; Guspanova, Jana; Imrich, Jan; Busova, Tatiana
Collection of Czechoslovak Chemical Communications, 1997 , vol. 62, # 9 p. 1491 - 1496
反应条件
tetrachloromethane; triethylamine in acetonitrile
T=20°C; Atherton-Todd reaction; 0.5 h;
参考文献
Shi, Enxue; Pei, Chengxin
Synthesis, 2004 , # 18 p. 2995 - 2998
反应条件
18-crown-6 ether in ethyl acetate
T=20°C;
参考文献
Shi, Enxue; Pei, Chengxin
Synthetic Communications, 2005 , vol. 35, # 5 p. 669 - 673
反应条件
alkali metal thiocyanide
T=60°C; 0.0166667 h; Microwave irradiationneat (no solvent);
参考文献
Shi, Enxue; Xiao, Junhua; Pei, Chengxin; Chen, Jisheng
Synthetic Communications, 2011 , vol. 41, # 20 p. 3085 - 3088
反应条件
O,O-(1,2-dimethylethylene) S-(trimethylsilyl) phosphorodithioate
360 h; Ambient temperature;
参考文献
Kutyrev, G. A.; Lygin, A. V.; Cherkasov, R. A.; Konovalova, I. V.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 6 p. 1213 - 1219,1080 - 1085
反应条件
diphenyl phosphoroisocyanatidate
360 h; Ambient temperature;
参考文献
Kutyrev, G. A.; Lygin, A. V.; Cherkasov, R. A.; Konovalova, I. V.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 6 p. 1213 - 1219,1080 - 1085
反应条件
in acetonitrile
T=55°C; Kinetics;
参考文献
Barai, Hasi Rani; Lee, Hai Whang
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 615 - 620
参考文献
Cates; Lemke
Journal of Pharmaceutical Sciences, 1974 , vol. 63, # 11 p. 1736 - 1739
反应条件
in acetonitrile
Ambient temperature;
参考文献
Cates; Lemke
Journal of Pharmaceutical Sciences, 1974 , vol. 63, # 11 p. 1736 - 1739