1-(3-硝基苯基)乙醇合成路线 （共 20 条）
反应条件
chloro-trimethyl-silane; 1,1-dimethylpropan-1-ol; sodium hydride; zinc(II) chloride in tetrahydrofuran T=63°C; 0.5 h;
参考文献
Fernandes, Jane Luiza Nogueira; De Souza, Marcos Costa; Brenelli, Eugenia Cristina Souza; Brenelli, Jose Afranio
Synthesis, 2009 , # 23 art. no. M03909SS, p. 4058 - 4062
反应条件
oxygen; TEAB; Co(TPP) in ethylene glycol dimethyl ether; isopropyl alcohol 72 h; Ambient temperature;
参考文献
Okamoto, Tadashi; Oka, Shinzaburo
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1589 - 1594
反应条件
in tetrahydrofuran; methanol
参考文献
Journal of the American Chemical Society, , vol. 71, p. 3622,3623
Chemische Berichte, , vol. 70, p. 1520,1524
反应条件
1: 3-chloro-benzenecarboperoxoic acid / chloroform / 2 h / Reflux 2: Candida tenuis AKR2B5 xylose reductase [E.(1)C11175]; water; Reduced nicotinamide-adenine dinucleotide / ethanol / 25 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 16 p. 5863 - 5870
反应条件
CuF(PPh3)3*2MeOH; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=20°C; Aldol Addition; 2 h; Inert atmosphereSchlenk technique; diastereoselective reaction;
参考文献
Li, Zengchang; Jiang, Lan; Li, Zhengning; Chen, Huiying
Chinese Journal of Chemistry, 2013 , vol. 31, # 4 p. 539 - 544
反应条件
water in 2,2,2-trifluoroethanol T=25°C; Kinetics;
参考文献
Organic Letters, , vol. 6, # 20 p. 3633 - 3636
反应条件
in diethyl ether Heating;
参考文献
Hatzakis, Nikos S.; Smonou, Ioulia
Bioorganic Chemistry, 2005 , vol. 33, # 4 p. 325 - 337
反应条件
1: aq. HBr / acetic acid 2: ethanol 3: aq. H2SO4 4: H2 / Raney-Ni / ethanol 5: KICl2, aq. HCl View Scheme
参考文献
Felder; Pitre; Fumagalli; Lorenzotti
Journal of medicinal chemistry, 1970 , vol. 13, # 3 p. 559 - 561
反应条件
1: aq. HBr / acetic acid 2: ethanol 3: aq. H2SO4 4: H2 / Raney-Ni / ethanol 5: KICl2, aq. HCl 6: (i) H2SO4, (ii) aq. NaOH View Scheme
参考文献
Felder; Pitre; Fumagalli; Lorenzotti
Journal of medicinal chemistry, 1970 , vol. 13, # 3 p. 559 - 561
