2,4,6-三氯-3-甲基-苯胺合成路线 （共 10 条）
参考文献
Cohen; Dakin
Journal of the Chemical Society, 1902 , vol. 81, p. 1335
Journal of the Chemical Society, 1906 , vol. 89, p. 1454
参考文献
Morley,J.S.
Journal of the Chemical Society, 1961 , p. 1414 - 1416
反应条件
1: CH3SO3H / Heating 2: sodium formate / 5percent Pd/C / acetonitrile / 24 h / Heating 3: 90 percent / aq. HCl / acetic acid View Scheme
参考文献
Pews; Hunter; Wehmeyer
Tetrahedron Letters, 1991 , vol. 32, # 49 p. 7191 - 7194
反应条件
1: CH3SO3H / Heating 2: sodium formate / 5percent Pd/C / acetonitrile / 24 h / Heating View Scheme
参考文献
Pews; Hunter; Wehmeyer
Tetrahedron Letters, 1991 , vol. 32, # 49 p. 7191 - 7194
反应条件
1: aq.-ethanolic hydrochloric acid; sodium nitrite / unter Kuehlung und anschliessenden Erhitzen mit Wasserdampf 2: chlorine / 80 °C / Irradiation View Scheme
参考文献
Piraux; Bruylants
Bulletin des Societes Chimiques Belges, 1959 , vol. 68, p. 491,496
参考文献
White; Adams
Journal of the American Chemical Society, 1932 , vol. 54, p. 2104,2107
反应条件
hydrogenchloride; chlorine in tetrachloromethane; ethanol
ice-bath;
参考文献
Pews; Hunter; Wehrmeyer
Tetrahedron, 1993 , vol. 49, # 22 p. 4809 - 4820
参考文献
Bures; Spitnikova
C.csl.Lekarn., 1937 , vol. 17, p. 189,194
Chem. Zentralbl., 1938 , vol. 109, # I p. 871
反应条件
1: hydrochloric acid; glacial acetic acid
2: sulfuric acid
View Scheme
参考文献
Cohen; Dakin
Journal of the Chemical Society, 1902 , vol. 81, p. 1335
Journal of the Chemical Society, 1906 , vol. 89, p. 1454
反应条件
Diazotization.Behandlung der Diazoniumchloridloesung mit CuCl;
参考文献
Bures; Trpisovska
C. csl. Lekarn., 1935 , vol. 15, p. 179
Chem. Zentralbl., 1936 , vol. 107, # I p. 1209
