2-(1,1-二甲基乙基)-1H-吡咯合成路线 (共 15 条)
反应条件
1: hydroxylamine hydrochloride; sodium acetate / water; ethanol / 20 °C
2: triethylamine / dichloromethane / 0 °C
3: copper(I) bromide / toluene / 120 °C / |Inert atmosphere
View Scheme
参考文献
Du, Wei; Zhao, Mi-Na; Ren, Zhi-Hui; Wang, Yao-Yu; Guan, Zheng-Hui
Chemical Communications, 2014 , vol. 50, # 56 p. 7437 - 7439
反应条件
1: triethylamine / dichloromethane / 0 °C
2: copper(I) bromide / toluene / 120 °C / |Inert atmosphere
View Scheme
参考文献
Du, Wei; Zhao, Mi-Na; Ren, Zhi-Hui; Wang, Yao-Yu; Guan, Zheng-Hui
Chemical Communications, 2014 , vol. 50, # 56 p. 7437 - 7439
反应条件
Yield given. Multistep reaction;
参考文献
Felkin, Hugh; Zakrzewski, Janusz
Journal of the American Chemical Society, 1985 , vol. 107, # 11 p. 3374 - 3375
反应条件
Amberlyst 15
T=80°C; 12 h; Yield given. Yields of byproduct given;
参考文献
Iovel, I.; Goldberg, Yu.; Shymanska, M.; Lukevics, E.
Synthetic Communications, 1988 , vol. 18, # 11 p. 1261 - 1266
反应条件
oxygen; trimethylamine
T=37.5°C; Irradiation; Product distribution;
参考文献
Speranza, Maurizio
Journal of the Chemical Society, Chemical Communications, 1981 , # 22 p. 1177 - 1178