二苯并[b,d]呋喃-2-甲醛合成路线 （共 7 条）
参考文献
Sengupta, Dibyendu; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 72 - 75
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane 10 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, # 12 p. 4464 - 4466
反应条件
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 0 - 20 °C 2: potassium hydroxide / methanol / 2 h / 20 °C View Scheme
参考文献
Yempala, Thirumal; Sridevi, Jonnalagadda Padma; Yogeeswari, Perumal; Sriram, Darmarajan; Kantevari, Srinivas
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 19 p. 5393 - 5396
反应条件
dibenzoyl peroxide in methanol; sulfuric acid
T=40°C; 48 h;
参考文献
Fujishiro, Koichi; Mitamura, Shuichi
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 12 p. 4464 - 4466
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
10 h; Ambient temperature;
参考文献
Fujishiro, Koichi; Mitamura, Shuichi
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 12 p. 4464 - 4466
反应条件
1.1: sodium tetrahydroborate / tetrahydrofuran / 2 h / 20 °C
1.2: 0.33 h / 20 °C
2.1: thionyl chloride / dichloromethane / 0.33 h / 80 °C / Microwave irradiation
View Scheme
参考文献
ExonHit Therapeutics SA; ALLERGAN, INC.
Patent: US2012/214837 A1, 2012 ;
US 20120214837 A1
反应条件
1: With sodium tetrahydroborate in tetrahydrofuran
T=20°C; 2 h;
2: With hydrogenchloride in tetrahydrofuran; water
T=20°C; 0.333333 h;
参考文献
ExonHit Therapeutics SA; ALLERGAN, INC.
Patent: US2012/214837 A1, 2012 ;
Location in patent: Page/Page column 26 ;
US 20120214837 A1
