四氢-2H-吡喃-2-甲腈合成路线 （共 10 条）
反应条件
tin(IV) chloride in dichloromethane
4 h; Ambient temperature;
参考文献
Reetz, Manfred T.; Chatziiosifidis, Ioannis; Kuenzer, Hermann; Mueller-Starke, Hans
Tetrahedron, 1983 , vol. 39, # 6 p. 961 - 966
反应条件
silver nitrate in water; dimethyl sulfoxide
T=110°C; 3 h;
参考文献
Mitani, Michiharu; Takeuchi, Hiroshi; Koyama, Kikuhiko
Chemistry Letters, 1987 , p. 333 - 334
反应条件
1: 3,4-dihydro-2H-pyran With hydrogenchloride in diethyl ether; dichloromethane
T=-40°C; 0.0833333 h; Inert atmosphere;
2: trimethylsilyl cyanide in dichloromethane
T=-40°C; 1 h; Inert atmosphere;
参考文献
Lu, Chunliang; Su, Xiaoge; Floreancig, Paul E.
Journal of Organic Chemistry, 2013 , vol. 78, # 18 p. 9366 - 9376
反应条件
tin(IV) chloride in dichloromethane
4 h; Ambient temperature;
参考文献
Reetz, Manfred T.; Chatziiosifidis, Ioannis; Kuenzer, Hermann; Mueller-Starke, Hans
Tetrahedron, 1983 , vol. 39, # 6 p. 961 - 966
反应条件
tin(ll) chloride in dichloromethane
Ambient temperature;
参考文献
Utimoto, Kiitiro; Wakabayashi, Yukio; Horiie,Takafumi; Inoue, Masaharu; Shishiyama, Yuho; et al.
Tetrahedron, 1983 , vol. 39, # 6 p. 967 - 974
反应条件
T=-10°C; Einleiten von Chlorwasserstoff und Erwaermen des Reaktionsgemisches mit Silbercyanid in Aether;
参考文献
Nelson et al.
Journal of the American Chemical Society, 1956 , vol. 21, p. 798
反应条件
in diethyl ether
3 h; Heating;
参考文献
Booth, Harold; Dixon, J. Mark; Khedhair, Khedhair A.
Tetrahedron, 1992 , vol. 48, # 29 p. 6161 - 6174
参考文献
Zelinski; Yorka
Journal of Organic Chemistry, 1958 , vol. 23, p. 640
参考文献
Zelinski; Yorka
Journal of Organic Chemistry, 1958 , vol. 23, p. 640
反应条件
1: 90 percent / LDA / tetrahydrofuran
2: 57 percent / tetraethylammonium p-toluenesulfonate / acetonitrile / zinc cathode; carbon rod anode; 3.0 F/mol
View Scheme
参考文献
Shono, Tatsuya; Terauchi, Jun; Kitayama, Kenji; Takeshima, Yo-Ichiro; Masumura, Yoshihiro
Tetrahedron, 1992 , vol. 48, # 38 p. 8253 - 8262
