反应条件
n-butyllithium in diethyl ether; hexane
byproducts: 2,6-(MeO)2C6H3SH; Ar-atmosphere; stirring slight excess of toluene derivative (in Et2O) with BuLi (in hexane) at room temp. for 2 h, addn. 0.22 equiv. of Sb-compd., stirring (room temp., 6 h); quenching with MeOH, filtration, crystn. on concn. (reduced pressure), recrystn. (Me2CO);
参考文献
Wada, Masanori; Natsume, Satoko; Suzuki, Shinobu; Uo, Akira; Nakamura, Michiaki; Hayase, Shuichi; Erabi, Tatsuo
Journal of Organometallic Chemistry, 1997 , vol. 548, # 2 p. 223 - 227
