4-(2,5-二甲基-苯基)-4-羰基-丁酸合成路线 （共 7 条）
反应条件
aluminium trichloride Heating;
参考文献
Mahmoodi; Jazayri
Synthetic Communications, 2001 , vol. 31, # 10 p. 1467 - 1475
反应条件
potassium hydroxide in ethanol
参考文献
Bulletin de la Societe Chimique de France, , p. 3023 - 3031
反应条件
1: AlCl3 2: KOH / ethanol View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 3023 - 3031
反应条件
carbon disulfide; aluminium trichloride Zersetzen des entstandenen Chlorids mit Wasser;
参考文献
Chemische Berichte, , vol. 20, p. 1375
反应条件
potassium hydroxide; hydrazine hydrate in various solvent(s) 1) 2 h, reflux, 2) 180-190 deg C, ca. 4 h;
参考文献
Boberg, Friedrich; Jachiewicz, Adam; Garming, Alfons
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 72, # 1-4 p. 1 - 12
反应条件
1: 70 percent / K2CO3 / acetone / Heating
2: 76 percent / hydrazine hydrate; CH3COONa / methanol / Heating
View Scheme
参考文献
Khan; Siddiqui
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2000 , vol. 39, # 8 p. 614 - 619
反应条件
1: 94 percent / 80percent N2H4*H2O, KOH / various solvent(s) / 1) 2 h, reflux, 2) 180-190 deg C, ca. 4 h
2: 68 percent / 80percent H2SO4 / 2 h / 100 °C
View Scheme
参考文献
Ruzicka; Waldmann
Helvetica Chimica Acta, 1932 , vol. 15, p. 907,914
