1-(4-溴苯基)-1-乙醇合成路线 （共 105 条）
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of the American Chemical Society, , vol. 71, p. 1675,1678
参考文献
Journal of the American Chemical Society, , vol. 71, p. 3622,3623
反应条件
Montmorillonite-K10; water T=80°C;
参考文献
Journal of Organic Chemistry, , vol. 73, # 18 p. 7365 - 7368
反应条件
C68H88Cl4Ir2N6NiO2; potassium tert-butylate in isopropyl alcohol T=80°C; 24 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 39 p. 11041 - 11051
反应条件
1.1: sulfuric acid; copper; copper(II) sulfate; potassium bromide / water / 2 h / Reflux 1.2: 80 - 90 °C 2.1: Candida tenuis AKR2B5 xylose reductase [E.(1)C11175]; water; Reduced nicotinamide-adenine dinucleotide / ethanol / 25 °C / pH 7 / aq. phosphate buffer; Enzymatic reaction View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 16 p. 5863 - 5870
反应条件
CuF(PPh3)3*2MeOH; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=20°C; Aldol Addition; 1 h; Inert atmosphereSchlenk technique; diastereoselective reaction;
参考文献
Li, Zengchang; Jiang, Lan; Li, Zhengning; Chen, Huiying
Chinese Journal of Chemistry, 2013 , vol. 31, # 4 p. 539 - 544
反应条件
CuF(PPh3)3*2MeOH; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=20°C; Aldol Addition; 1 h; Inert atmosphereSchlenk technique; diastereoselective reaction;
参考文献
Li, Zengchang; Jiang, Lan; Li, Zhengning; Chen, Huiying
Chinese Journal of Chemistry, 2013 , vol. 31, # 4 p. 539 - 544
反应条件
1: diethylzinc With C56H43N2OP in toluene T=-35°C; 0.5 h; Inert atmosphere; 2: para-bromoacetophenone in toluene T=-65°C; 96 h; Inert atmosphere; enantioselective reaction;
参考文献
Dalton Transactions, , vol. 42, # 40 p. 14576 - 14582
反应条件
[RuH(PN3P)(CO)]; isopropyl alcohol T=82°C; 16 h; Inert atmosphere;
参考文献
Journal of Organometallic Chemistry, , vol. 700, p. 202 - 206
反应条件
1.1: diethyl ether / -78 - 20 °C 2.1: dihydrogen peroxide; sulfuric acid / tetrahydrofuran; water / 24 h / 0 - 60 °C 3.1: copper diacetate; 1,10-phenanthroline; triethylamine; oxygen / toluene; acetonitrile / 20 °C 3.2: 1 h / 0 - 20 °C View Scheme
参考文献
Beilstein Journal of Organic Chemistry, , vol. 9, p. 1217 - 1225
