1-(4-溴苯基)-1-乙醇合成路线 （共 105 条）
反应条件
Benzoic acid (S)-1-[(S)-5-oxo-2-phenyl-3-(toluene-4-sulfonyl)-[1,3,2]oxazaborolidin-4-yl]-ethyl ester in diethyl ether T=-10°C; Mukaiyama reaction; 97 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Organic Letters, , vol. 10, # 21 p. 4991 - 5001
反应条件
oxygen; TEAB; Co(TPP) in ethylene glycol dimethyl ether; isopropyl alcohol 60 h; Ambient temperature;
参考文献
Okamoto, Tadashi; Oka, Shinzaburo
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1589 - 1594
反应条件
tin(ll) chloride in methanol 0.05 h; microwave irradiation;
参考文献
Gogoi, Dipankoj; Baruah, Nabajyoti; Bez, Ghanashyam
Synthetic Communications, 2007 , vol. 37, # 4 p. 595 - 599
反应条件
Benzoic acid (S)-1-[(S)-5-oxo-2-phenyl-3-(toluene-4-sulfonyl)-[1,3,2]oxazaborolidin-4-yl]-ethyl ester in diethyl ether T=-40°C; Mukaiyama reaction; 24 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Organic Letters, , vol. 10, # 21 p. 4991 - 5001
反应条件
(1-azabicyclo{2.2.2}octane)aluminium hydride in toluene 16 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 35, # 32 p. 5915 - 5918
反应条件
Benzoic acid (S)-1-[(S)-5-oxo-2-phenyl-3-(toluene-4-sulfonyl)-[1,3,2]oxazaborolidin-4-yl]-ethyl ester in dichloromethane T=-40°C; Mukaiyama reaction; 24 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Organic Letters, , vol. 10, # 21 p. 4991 - 5001
反应条件
(2,6-t-Bu2-4-Me-C6H2O)2AlMe; diisobutylaluminium hydride T=-78°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 110, # 8 p. 2650 - 2652
反应条件
potassium fluoride; tetrabutyl ammonium fluoride in dichloromethane T=65°C; 1 h;
参考文献
Fritz-Langhals, Elke
Tetrahedron Letters, 1994 , vol. 35, # 12 p. 1851 - 1854
反应条件
cesium fluoride in dichloromethane T=65°C; 1 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 35, # 12 p. 1851 - 1854
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; iron(II) oxalate dihydrate T=155 - 160°C; 0.5 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 1, # 10 p. 1737 - 1740
