反应条件
1: 1,3-bis-(1-hydroxy-1-trifluoromethyl-2,2,2-trifluoroethyl)-benzene With sodium hydride in N,N-dimethyl-formamide
T=-20 - -10°C;
2: methanesulphonic acid methyl ester in N,N-dimethyl-formamide
T=20°C; 12 h;
参考文献
Rabai, Jozsef; Szabo, Denes; Borbas, Eszter K.; Koevesi, Istvan; Koevesdi, Istvan; Csampai, Antal; Goemoery, Agnes; Pashinnik, Valeriy E.; Shermolovich, Yuriy G.
Journal of Fluorine Chemistry, 2002 , vol. 114, # 2 p. 199 - 207
