反应条件
1: thionyl chloride
2: triethylamine / dichloromethane / 5 h / 0 °C
3: 2,5,7,8-tetramethyl-2-(4',8',12'-trimethyltridecyl)-6-chromanol; potassium tert-butylate / dimethyl sulfoxide / 3 h / 100 °C / |Inert atmosphere
View Scheme
参考文献
Kumar, Sangit; Bhakuni, Bhagat Singh; Yadav, Abhimanyu; Kumar, Shailesh; Patel, Saket; Sharma, Shubham
Journal of Organic Chemistry, 2014 , vol. 79, # 7 p. 2944 - 2954