1-甲基-1H-吡啶并[2,3-d][1,3]噁嗪-2,4-二酮合成路线 (共 5 条)
反应条件
sodium hydride in N,N-dimethyl-formamide 3 h; Ambient temperature;
参考文献
Canonne, P.; Boulanger, R.; Chantegrel, B.
Tetrahedron, 1987 , vol. 43, # 4 p. 663 - 668
反应条件
1: 75 percent / lead tetra-acetate / dimethylformamide 2: 80 percent / sodium hydride / dimethylformamide / 3 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 43, # 4 p. 663 - 668
参考文献
Journal of Heterocyclic Chemistry, , vol. 16, # 4 p. 829 - 830
反应条件
sodium hydride 1) dimethylacetamide, 2) 120 deg C, 18 h; Yield given. Multistep reaction;
参考文献
American Home Products Corporation
Patent: US4347362 A1, 1982 ;
反应条件
sodium hydride
1) dimethylacetamide, RT, 30 min, 2) 120 deg C, 18 h; Yield given. Multistep reaction;
参考文献
Coppola, Gary M.; Fraser, James D.; Hardtmann, Goetz E.; Shapiro, Michael J.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 193 - 206