1-(二溴甲基)-3-苯氧基苯合成路线 （共 5 条）
反应条件
dipotassium peroxodisulfate; lithium bromide in acetic acid
T=113°C; 6 h;
参考文献
Citterio, Attilio; Santi, Roberto; Pagani, Anselmo
Journal of Organic Chemistry, 1987 , vol. 52, # 22 p. 4925 - 4927
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane
T=78°C; 6 h; Yield given. Yields of byproduct given;
参考文献
Shapiro, E. A.; Eismont, M. Yu.; Pereverzeva, Yu. O.; Nefedov, A. O.; Srashnenko, A. V.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 3.2 p. 573 - 577
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 3 p. 652 - 656
参考文献
Toyo Soda Manufacturing Co., Ltd.
Patent: US4393246 A1, 1983 ;
反应条件
1: 61 percent / Cu, NaOH, KOH / 5 h / 220 °C
2: NBS, azobisisobutyronitrile / CCl4 / 6 h / 78 °C
View Scheme
参考文献
Shapiro, E. A.; Eismont, M. Yu.; Pereverzeva, Yu. O.; Nefedov, A. O.; Srashnenko, A. V.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 3.2 p. 573 - 577
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 3 p. 652 - 656
反应条件
1: 61 percent / Cu, NaOH, KOH / 5 h / 220 °C
2: NBS, azobisisobutyronitrile / CCl4 / 6 h / 78 °C
View Scheme
参考文献
Shapiro, E. A.; Eismont, M. Yu.; Pereverzeva, Yu. O.; Nefedov, A. O.; Srashnenko, A. V.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 3.2 p. 573 - 577
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 3 p. 652 - 656
