三环[9.2.2.1(4,8)]十六碳-4,6,8(16),11,13,14-六烯合成路线 (共 19 条)
反应条件
T=930°C; P=0.1 Torr; detected by 13C nmr; Product distributionMechanism;
参考文献
Chapman, Orville L.; Tsou, Uh-Po Eric; Johnson, Jeffery W.
Journal of the American Chemical Society, 1987 , vol. 109, # 2 p. 553 - 559
反应条件
T=930°C; P=0.1 Torr; detected by 13C nmr; Product distributionMechanism;
参考文献
Chapman, Orville L.; Tsou, Uh-Po Eric; Johnson, Jeffery W.
Journal of the American Chemical Society, 1987 , vol. 109, # 2 p. 553 - 559
反应条件
T=930°C; P=0.1 Torr; detected by 13C nmr; Product distributionMechanism;
参考文献
Chapman, Orville L.; Tsou, Uh-Po Eric; Johnson, Jeffery W.
Journal of the American Chemical Society, 1987 , vol. 109, # 2 p. 553 - 559
反应条件
in benzene
5 h; Ambient temperatureIrradiation;
参考文献
Isaji, Hajime; Yasutake, Mikio; Takemura, Hiroyuki; Sako, Katsuya; Tatemitsu, Hitoshi; Inazu, Takahiko; Shinmyozu, Teruo
European Journal of Organic Chemistry, 2001 , # 13 p. 2487 - 2499
反应条件
aluminium trichloride; nitromethane in benzene
T=50°C; 1.5 h;
参考文献
Yamato, Takehiko; Matsumoto, Jun-ichi; Tokuhisa, Kiwamu; Tsuji, Katsuya; Suehiro, Kazuaki; Tashiro, Masashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 20 p. 2675 - 2682
反应条件
n-butyllithium in diethyl ether; hexane
参考文献
Sherrod,S.A. et al.
Journal of the American Chemical Society, 1974 , vol. 96, p. 1565 - 1577
反应条件
potassium hydroxide; sodium disulfite in ethanol; water
Heating;
参考文献
Takemura, Hiroyuki; Shinmyozu, Teruo; Inazu, Takahiko
Tetrahedron Letters, 1988 , vol. 29, # 9 p. 1031 - 1032
反应条件
hydrogenchloride; aluminium trichloride in dichloromethane
参考文献
Hefelfinger,D.T.; Cram,D.J.
Journal of the American Chemical Society, 1971 , vol. 93, p. 4754 - 4767
反应条件
hydrogen; palladium on activated charcoal
参考文献
Boekelheide,V. et al.
Journal of the American Chemical Society, 1974 , vol. 96, # 5 p. 1558 - 1564
反应条件
1: 500 °C / 1.2 Torr
2: nBuLi / diethyl ether; hexane
View Scheme
参考文献
Sherrod,S.A. et al.
Journal of the American Chemical Society, 1974 , vol. 96, p. 1565 - 1577