(2-甲基-1-苯并呋喃-3-基)甲醇合成路线 （共 5 条）
反应条件
hydrogenchloride in tetrahydrofuran; water
T=60°C; 2 h;
参考文献
Luo, Huan; Liu, Yan-Fei; Zhang, Chun-Lei; Wang, Yan; Ni, Gang; Yu, De-Quan
Chinese Chemical Letters, 2013 , vol. 24, # 12 p. 1115 - 1117
反应条件
lithium aluminium tetrahydride in diethyl ether
10 h; Ambient temperature;
参考文献
Chou, Chin-Hsing; Trahanovsky, Walter S.
Journal of Organic Chemistry, 1986 , vol. 51, # 22 p. 4208 - 4212
反应条件
4 A molecular sieve; tetrabutyl ammonium fluoride in tetrahydrofuran
T=50°C; Yields of byproduct given;
参考文献
Ito, Yasuko; Aoyama, Toyohiko; Shioiri, Takayuki
Synlett, 1997 , vol. 1997, # 10 p. 1163 - 1164
反应条件
1: 1.) n-BuLi / 1.) THF, from -78 to 0 deg C, 1 h, 2.) THF, RT, overnight
2: 92 percent / LiAlH4 / diethyl ether / 10 h / Ambient temperature
View Scheme
参考文献
Chou, Chin-Hsing; Trahanovsky, Walter S.
Journal of Organic Chemistry, 1986 , vol. 51, # 22 p. 4208 - 4212
反应条件
1: 81.6 percent / 700 °C / 0 Torr
2: 1.) n-BuLi / 1.) THF, from -78 to 0 deg C, 1 h, 2.) THF, RT, overnight
3: 92 percent / LiAlH4 / diethyl ether / 10 h / Ambient temperature
View Scheme
参考文献
Chou, Chin-Hsing; Trahanovsky, Walter S.
Journal of Organic Chemistry, 1986 , vol. 51, # 22 p. 4208 - 4212
