5,6-二氨基-2-吡啶羧酸甲酯合成路线 （共 4 条）
反应条件
hydrogen; platinum(IV) oxide in ethanol P=1551.44 Torr; 0.5 h;
参考文献
Chand, Pooran; Kotian, Pravin L.; Morris, Philip E.; Bantia, Shanta; Walsh, David A.; Babu, Yarlagadda S.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 7 p. 2665 - 2678
反应条件
1: 61 percent / Pd(OAc)2; Ph3P; Et3N / dimethylformamide / 15 h / 60 °C / 11400 Torr 2: 79 percent / H2 / Pd/C / methanol; ethyl acetate / 4 h View Scheme
参考文献
Journal of the American Chemical Society, , vol. 125, # 19 p. 5707 - 5716
反应条件
1: 0.40 g / sulfuric acid / 4 h / Heating 2: 96 percent / H2 / platinum(IV) oxide / ethanol / 0.5 h / 1551.44 Torr View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 7 p. 2665 - 2678
反应条件
1: 38.5 percent / dimethylformamide / 16 h / 140 °C 2: 1.8 g / potassium carbonate; potassium permanganate / H2O; 2-methyl-propan-2-ol / 3 h 3: 0.40 g / sulfuric acid / 4 h / Heating 4: 96 percent / H2 / platinum(IV) oxide / ethanol / 0.5 h / 1551.44 Torr View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 7 p. 2665 - 2678
