6-氨基-5-硝基-2-吡啶羧酸甲酯合成路线 (共 5 条)
反应条件
palladium diacetate; triethylamine; triphenylphosphine in N,N-dimethyl-formamide T=60°C; P=11400 Torr; 15 h;
参考文献
Renneberg, Dorte; Dervan, Peter B.
Journal of the American Chemical Society, 2003 , vol. 125, # 19 p. 5707 - 5716
反应条件
1: 38.5 percent / dimethylformamide / 16 h / 140 °C 2: 1.8 g / potassium carbonate; potassium permanganate / H2O; 2-methyl-propan-2-ol / 3 h 3: 0.40 g / sulfuric acid / 4 h / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 7 p. 2665 - 2678
反应条件
sulfuric acid 4 h; Heating;
参考文献
Chand, Pooran; Kotian, Pravin L.; Morris, Philip E.; Bantia, Shanta; Walsh, David A.; Babu, Yarlagadda S.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 7 p. 2665 - 2678
反应条件
hydrogen; platinum(IV) oxide in ethanol P=1551.44 Torr; 0.5 h;
参考文献
Chand, Pooran; Kotian, Pravin L.; Morris, Philip E.; Bantia, Shanta; Walsh, David A.; Babu, Yarlagadda S.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 7 p. 2665 - 2678
反应条件
hydrogen in palladium monocarbide
参考文献
California Institute of Technology
Patent: US2005/26174 A1, 2005 ;