N-(3-丁炔-2-基)苯胺合成路线 （共 13 条）
反应条件
copper(l) chloride in tetrahydrofuran
T=50°C; 2 h;
参考文献
Imada, Yasushi; Yuasa, Mari; Nakamura, Ishin; Murahashi, Shun-Ichi
Journal of Organic Chemistry, 1994 , vol. 59, # 9 p. 2282 - 2284
反应条件
potassium in 1,4-dioxane
T=150°C; P=9120 Torr; 10 h; in autoclave;
参考文献
Trofimov, B. A.; Malysheva, S. F.; Vyalykh, E. P.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 1405 - 1409
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 8 p. 1583 - 1587
反应条件
potassium in 1,4-dioxane
T=150°C; P=9120 Torr; 10 h; in autoclave;
参考文献
Trofimov, B. A.; Malysheva, S. F.; Vyalykh, E. P.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 1405 - 1409
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 8 p. 1583 - 1587
反应条件
potassium in 1,4-dioxane
T=160°C; P=9120 Torr; 2 h; in autoclave;
参考文献
Trofimov, B. A.; Malysheva, S. F.; Vyalykh, E. P.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 1405 - 1409
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 8 p. 1583 - 1587
反应条件
in ethylene glycol dimethyl ether
T=100°C; Strecker reaction; 0.166667 h; AutoclaveMicrowave irradiation;
参考文献
Gising, Johan; Oertqvist, Pernilla; Sandstroem, Anja; Larhed, Mats
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 13 p. 2809 - 2815
反应条件
copper(I) monacetylide; benzene
T=125 - 130°C; P=14710.2 Torr;
参考文献
Wolf; Ramin
Justus Liebigs Annalen der Chemie, 1959 , vol. 626, p. 47,49
反应条件
1: aniline With potassium carbonate in N,N-dimethyl-formamide
T=25°C; 0.0833333 h;
2: methyl propargyl bromide in N,N-dimethyl-formamide; toluene
T=25°C; 6 h;
参考文献
Chen, Yu; Dubrovskiy, Anton; Larock, Richard C.
Organic Syntheses, 2012 , vol. 89, p. 294 - 306
反应条件
sodium hydride in N,N-dimethyl-formamide
6 h; Ambient temperature;
参考文献
Ramana; Sudha
Journal of Mass Spectrometry, 1995 , vol. 30, # 7 p. 1028 - 1033
反应条件
potassium in 1,4-dioxane
T=150°C; P=9120 Torr; 2 h; other solvent; other temperature; other time; Product distributionMechanism;
参考文献
Trofimov, B. A.; Malysheva, S. F.; Vyalykh, E. P.
Journal of Organic Chemistry USSR (English Translation), 1981 , p. 1405 - 1409
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 8 p. 1583 - 1587
反应条件
1: 80 percent / diethyl ether / 0.5 h / Ambient temperature
2: 73 percent / KF / dimethylformamide / 1.5 h / Ambient temperature
View Scheme
参考文献
Suvorova, I. V.; Khramchikhin, A. V.; Stadnichuk, M. D.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 7 p. 1588 - 1591,1415 - 1417
