4-甲酰基氨基噻吩-3-羧酸甲酯合成路线 (共 7 条)
反应条件
1: DMAP / acetonitrile 2: NaOMe / methanol 3: LiOH / tetrahydrofuran; H2O View Scheme
参考文献
Carroll, William A.; Zhang, Xiaolin
Tetrahedron Letters, 1997 , vol. 38, # 15 p. 2637 - 2640
反应条件
1: DMAP / acetonitrile 2: NaOMe / methanol View Scheme
参考文献
Carroll, William A.; Zhang, Xiaolin
Tetrahedron Letters, 1997 , vol. 38, # 15 p. 2637 - 2640
反应条件
sodium acetate in water
T=20 - 55°C; 3.5 h;
参考文献
Shin, Dongwon; Sinkeldam, Renatus W.; Tor, Yitzhak
Journal of the American Chemical Society, 2011 , vol. 133, # 38 p. 14912 - 14915
反应条件
formic acid; NaOAc·3H2O
参考文献
Agrevo UK Limited
Patent: US6432964 B1, 2002 ;
参考文献
Baker et al.
Journal of Organic Chemistry, 1953 , vol. 18, p. 133,136
反应条件
1: barium carbonate; methanol; hydroxylamine hydrochloride / Behandeln einer Loesung des erhaltenen Oxims (Oel) in Aether mit Chlorwasserstoff enthaltendem Methanol
2: sodium acetate
View Scheme
参考文献
Baker et al.
Journal of Organic Chemistry, 1953 , vol. 18, p. 133,136
参考文献
Carroll, William A.; Zhang, Xiaolin
Tetrahedron Letters, 1997 , vol. 38, # 15 p. 2637 - 2640