3-[1,3,4]噁二唑-2-苯胺合成路线 (共 4 条)
反应条件
palladium 10 on activated carbon; hydrogen in methanol T=20°C; 16 h;
参考文献
AGIOS PHARMACEUTICALS, INC.; Popovici-Muller, Janeta; SAUNDERS, Jeffrey, O.; SALITURO, Francesco, G.; CAI, Zhenwei; YAN, Shunqi; ZHOU, Ding
Patent: WO2013/107405 A1, 2013 ;
Location in patent: Paragraph 65 ;
反应条件
hydrogen; palladium on activated charcoal in methanol P=760 Torr; 1 h; Ambient temperature;
参考文献
Bulletin de la Societe Chimique de France, , p. 1587 - 1591
反应条件
in chloroform T=20°C; 12.25 h;
参考文献
Ramazani, Ali; Souldozi, Ali
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 12 p. 3191 - 3198
反应条件
1: xylene / 6.7 h / Heating 2: H2 / Pd-C / methanol / 1 h / 760 Torr / Ambient temperature View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 1587 - 1591