1-苯并噻吩-5-基异氰酸酯合成路线 （共 15 条）
反应条件
in water T=150°C; 3 h;
参考文献
Galons, Herve; Bergerat, Isabelle; Combet Farnoux, Claude; Miocque, Marcel
Synthesis, 1982 , # 12 p. 1103 - 1105
反应条件
sodium tetrahydroborate in methanol T=0°C; 2.5 h;
参考文献
Kleyi, Phumelele; Walmsley, Ryan S.; Gundhla, Isaac Z.; Walmsley, Tara A.; Jauka, Tembisa I.; Dames, Joanna; Walker, Roderick B.; Torto, Nelson; Tshentu, Zenixole R.
South African Journal of Chemistry, 2012 , vol. 65, p. 231 - 238
反应条件
1: 1.) n-BuLi / 1.) Et2O, hexane, -45 deg C, 30 min, 2 a.) -75 deg C, b.) 0 deg C, 10 min 2: NaBH4 / methanol / 2.5 h / 0 °C View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 33, # 2 p. 781 - 789
反应条件
sodium acetate in water; acetic acid T=140°C; 12 h;
参考文献
Journal of Organic Chemistry, , vol. 54, # 6 p. 1256 - 1264
反应条件
1: ethanol; aqueous HCl 2: aqueous HNO3 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 71, p. 383,384
反应条件
1: aqueous HNO3 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 71, p. 383,384
反应条件
1: potassium hydroxide / acetone / 2 h 2: sodium tetrahydroborate / methanol / 2.5 h / 0 °C View Scheme
参考文献
South African Journal of Chemistry, , vol. 65, p. 231 - 238
反应条件
selenium(IV) oxide in 1,4-dioxane
参考文献
Odzak, Renata; Skocibusic, Mirjana; Maravic, Ana
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 23 p. 7499 - 7506
反应条件
1: selenium(IV) oxide / 1,4-dioxane 2: hydroxylamine hydrochloride / ethanol / pH 7 - 8 View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 21, # 23 p. 7499 - 7506
反应条件
thionyl chloride in chloroform 2 h; Heating;
参考文献
Birker, Paul J. M. W. L.; Godefroi, Eric F.; Helder, Janneke; Reedijk, Jan
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7556 - 7560
