N,N-二甲氧基羰基乙基苯胺合成路线 (共 5 条)
反应条件
in hexafluoroisopropyl alcohol T=58°C; Aza-Michael reaction; 12 h;
参考文献
De, Kavita; Legros, Julien; Crousse, Benoit; Bonnet-Delpon, Daniele
Journal of Organic Chemistry, 2009 , vol. 74, # 16 p. 6260 - 6265
反应条件
aluminum oxide T=100 - 110°C; 3 h;
参考文献
Tetrahedron, , vol. 70, # 14 p. 2449 - 2454
反应条件
[bmim]BF4; copper acetylacetonate T=20°C; aza-Michael reaction; 0.25 h;
参考文献
Kantam, M. Lakshmi; Neeraja; Kavita; Neelima; Chaudhuri, Mihir K.; Hussain, Sahid
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 6 p. 763 - 766
反应条件
sodium hydroxide 5 h; Heating;
参考文献
Centore, Roberto; Carella, Antonio; Pugliese, Andrea; Sirigu, Augusto; Tuzi, Angela
Acta Crystallographica Section C: Crystal Structure Communications, 2006 , vol. 62, # 8 p. o531-o533
反应条件
1: With titanium tetrachloride in dichloromethane
T=-20 - -5°C; 2 h;
2: With triethylamine in dichloromethane
T=20°C; 18 h;
参考文献
Raghavan, Subharekha; Schmidt, Darby Rye; Colletti, Steven L.; Smenton, Abigail Lee
Patent: US2009/62269 A1, 2009 ;
Location in patent: Page/Page column 41 ;