(S)-(+)-1,2,3,4-四氢-1-萘酚合成路线 (共 60 条)
反应条件
dimethylsulfide borane complex; C21H35BO5 in tetrahydrofuran T=-78°C; 6 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Arkivoc, , vol. 2011, # 7 p. 128 - 135
反应条件
tris(hydroxymethyl)methylamine hydrochloride; sodium chloride; calcium chloride in water; acetonitrile T=25°C; pH=8; 96 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of the Brazilian Chemical Society, , vol. 22, # 2 p. 300 - 307
反应条件
1: With C38H31Cl2N3O4PRe in 1,4-dioxane T=20°C; 2: With tetrabutyl ammonium fluoride in 1,4-dioxane T=20°C; optical yield given as percent eeenantioselective reaction;
参考文献
Chemistry - A European Journal, , vol. 16, # 31 p. 9555 - 9562
反应条件
2-acetyloxy-1-propene; lipase YS in di-isopropyl ether T=30°C; 7 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 1253 - 1256
反应条件
potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate in tetrahydrofuran; methanol 16 h;
参考文献
Synthesis, , # 6 p. 925 - 931
反应条件
phospholipase A2 from the rattlesnake Crotalus durissus terrificus; tris(hydroxymethyl)methylamine hydrochloride; sodium chloride; calcium chloride in water; acetonitrile T=25°C; pH=8; 96 h; Enzymatic reaction; optical yield given as percent ee;
参考文献
Journal of the Brazilian Chemical Society, , vol. 22, # 2 p. 300 - 307
反应条件
(-)-Tetramisole; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=-78°C; 20 h; Inert atmosphereMolecular sieve; optical yield given as percent ee;
参考文献
Journal of Organic Chemistry, , vol. 77, # 7 p. 3570 - 3575
反应条件
lipase YS in di-isopropyl ether T=30°C; 7 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 1253 - 1256
反应条件
(-)-Tetramisole; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=-78°C; 20 h; Inert atmosphereMolecular sieve; optical yield given as percent ee;
参考文献
Journal of Organic Chemistry, , vol. 77, # 7 p. 3570 - 3575
反应条件
in water hydrolysis by a Rhizopus nigricans culture; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 22, # 27 p. 2527 - 2530