(S)-(+)-1,2,3,4-四氢-1-萘酚合成路线 (共 60 条)
反应条件
3 A molecular sieve; oxygen; (-)-sparteine; palladium dichloro (η-2,5-norbornadiene) in toluene T=80°C; P=760.051 Torr; 40 h;
参考文献
Journal of the American Chemical Society, , vol. 123, # 31 p. 7725 - 7726
反应条件
triethylammonium formate; chiral 'roofed' cis-diamine-Ru(II) T=25°C; 20 h;
参考文献
Teitelbaum, Aaron M.; Meissner, Anja; Harding, Ryan A.; Wong, Christopher A.; Aldrich, Courtney C.; Remmel, Rory P.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 17 p. 5605 - 5617
反应条件
water; Phaseolus aureus L (green grams) T=15 - 20°C; 24 h; Enzymatic reaction;
参考文献
COUNCIL OF SCIENTIFIC AND INDUSTRIAL RESEARCH
Patent: WO2004/87629 A1, 2004 ;
Location in patent: Page 5 ;
反应条件
sodium hydroxide; (R)-1-(2-diphenylphosphino-1-naphthyl)phenanthridine rhodium; dihydrogen peroxide; benzo[1,3,2]dioxaborole 1.) THF, RT, 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron: Asymmetry, , vol. 6, # 10 p. 2593 - 2596
反应条件
dimethylsulfide borane complex in tetrahydrofuran T=20°C; 2 h; enantioselective reaction;
参考文献
Hosoda, Naoya; Kamito, Hideaki; Takano, Miki; Takebe, Yoshitaka; Yamaguchi, Yoshitaka; Asami, Masatoshi
Tetrahedron, 2013 , vol. 69, # 11 p. 2509 - 2509
反应条件
quinidine salt of 2-carboxy-benzoyl derivative
参考文献
Journal of the Chemical Society, , p. 3300,3302
反应条件
potassium hydroxide in ethanol T=25°C; 18 h;
参考文献
Lin, Gialih; Liu, Hsiao-Chien
Tetrahedron Letters, 1995 , vol. 36, # 34 p. 6067 - 6068
反应条件
[bis(acetoxy)iodo]benzene; tetraethylammonium bromide; [Mn{CHCH2CHPhNCH[OC6H2(t-Bu)2]}2]Cl in water T=20°C; 1 h;
参考文献
Angewandte Chemie - International Edition, , vol. 42, # 9 p. 1042 - 1044
反应条件
Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 37, # 37 p. 6777 - 6780
反应条件
in water T=25°C; 72 h; by Helminthosporium species; Yield given;
参考文献
Holland, Herbert L.; Bergen, Eleanor J.; Chenchaiah, P. Chinna; Khan, Shaheer H.; Munoz, Benito; et al.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 502 - 507