反应条件
1: 1) NaH / 1) benzene, 30 min, 2) rt, 20 h
2: 81 percent / KOH / aq. ethanol / Ambient temperature
3: oxalyl chloride, DMF / benzene / 2 h
4: 1) sodium pyridine-2-thiolate N-oxide, DMAP, 2) 2-methylpropane-2-thiol / 1) benzene, reflux, 30 min, 2) irradiation, reflux, 1 h
View Scheme
参考文献
Ahmad-Junan, S. Asiah; Walkington, Andrew J.; Whiting, Donald A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 18 p. 2313 - 2320
