2-甲基-5-亚甲基己二酸合成路线 (共 9 条)
反应条件
T=120°C; 4 h; Product distribution / selectivity;
参考文献
Rohm and Haas Company
Patent: EP1970367 A2, 2008 ;
Location in patent: Page/Page column 6 ;
反应条件
sulfuric acid
T=120 - 130°C; und Anschliessende Verseifung mit Wasser;
参考文献
Crawford
Journal of the Society of Chemical Industry, London, 1947 , vol. 66, p. 156
反应条件
water
T=230°C; 1 h; sealed tube; Further byproducts given;
参考文献
Zil'berman, E. N.; Salov, V. N.; Krasnov, V. L.; Gredniger, M. V.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 1 p. 29 - 32
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 1 p. 33 - 37
反应条件
sodium hydroxide; isobutylnaphthalenesulfonate sodium
参考文献
Crawford
Journal of the Society of Chemical Industry, London, 1947 , vol. 66, p. 156
Full Text Show Details
Imp. Chem. Ind.
Patent: US2244487 , 1940 ;
参考文献
Albisetti et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 472,474
参考文献
Albisetti et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 472,474
反应条件
in solid
T=250°C; 3 h; other metal salts; var. temp.; Product distributionMechanism;
参考文献
Kudoh, Masaaki; Naruchi, Kiyoshi; Akutsu, Fumihiko; Miura, Masatoshi
Journal of the Chemical Society, Chemical Communications, 1992 , # 2 p. 105 - 106
反应条件
T=120°C; anschliessendes Verseifen mit Wasser;
参考文献
Crawford
Journal of the Society of Chemical Industry, London, 1947 , vol. 66, p. 156
反应条件
T=200°C; 2 h; other alkali and alkaline earth salts; var. temperatures; Product distributionMechanism;
参考文献
Akutsu, Fumihiko; Aoyagi, Kaoru; Nishimura, Nozomu; Kudoh, Masaaki; Kasashima, Yoshio; Inoki, Mari; Naruchi, Kiyoshi
Journal of the Chemical Society. Perkin Transactions 2, 1996 , vol. 5, p. 889 - 892