2-氨基-6-甲氧基苯甲酸合成路线 (共 42 条)
反应条件
palladium in ethanol
参考文献
Imperial Chemical Industries, PLC
Patent: US5599814 A1, 1997 ;
参考文献
Chemische Berichte, , vol. 94, p. 2295 - 2305
Journal of the American Chemical Society, , vol. 99, p. 3734 - 3744
反应条件
1: 58 percent / conc. H2SO4, sodium dichromate / 20 h / Ambient temperature 2: 90 percent / sodium hydrogen carbonate / acetone / 30 h / Heating 3: 73 percent / ethanol / 11 h / Heating 4: 16 g / H2 / 10percent Pd/C / methanol / 760 Torr 5: 5percent NaOH View Scheme
参考文献
Australian Journal of Chemistry, , vol. 33, # 12 p. 2777 - 2779
反应条件
1: 90 percent / sodium hydrogen carbonate / acetone / 30 h / Heating 2: 73 percent / ethanol / 11 h / Heating 3: 16 g / H2 / 10percent Pd/C / methanol / 760 Torr 4: 5percent NaOH View Scheme
参考文献
Australian Journal of Chemistry, , vol. 33, # 12 p. 2777 - 2779
反应条件
1: 73 percent / ethanol / 11 h / Heating 2: 16 g / H2 / 10percent Pd/C / methanol / 760 Torr 3: 5percent NaOH View Scheme
参考文献
Australian Journal of Chemistry, , vol. 33, # 12 p. 2777 - 2779
反应条件
1: 16 g / H2 / 10percent Pd/C / methanol / 760 Torr 2: 5percent NaOH View Scheme
参考文献
Australian Journal of Chemistry, , vol. 33, # 12 p. 2777 - 2779
反应条件
1: SnCl2*2H2O, aq. HCl 2: aq. NaOH View Scheme
参考文献
Journal of the American Chemical Society, , vol. 99, p. 3734 - 3744
反应条件
hydrogenchloride in tetrahydrofuran
参考文献
Journal of Organic Chemistry, , vol. 56, # 23 p. 6666 - 6671
反应条件
1: 1) t-BuLi / 1) THF, 2) r.t., 6 h 2: conc. HCl / tetrahydrofuran View Scheme
参考文献
Journal of Organic Chemistry, , vol. 56, # 23 p. 6666 - 6671
反应条件
1: 94 percent / tetrahydrofuran / 48 h / 50 °C 2: 1) t-BuLi / 1) THF, 2) r.t., 6 h 3: conc. HCl / tetrahydrofuran View Scheme
参考文献
Journal of Organic Chemistry, , vol. 56, # 23 p. 6666 - 6671