1: 2-amino-5-nitro-phenol With hydrogenchloride; sodium hydroxide; sodium nitrite in water
1 h; Cooling with ice;
2: ethyl acetoacetate With sodium acetate in ethanol; water
T=0°C; Japp-Klingemann reaction; pH=8 - 10;
参考文献
Kopylovich, Maximilian N.; Mahmudov, Kamran T.; Da Silva, M. Fatima C. Guedes; Figiel, Pawel J.; Karabach, Yauhen Yu.; Kuznetsov, Maxim L.; Luzyanin, Konstantin V.; Pombeiro, Armando J.L.
Inorganic Chemistry, 2011 , vol. 50, # 3 p. 918 - 931
