1,2-苯并异噻唑-5-胺合成路线 (共 4 条)
反应条件
water; iron; acetic acid in ethyl acetate T=65°C; 1 h;
参考文献
N.V. Organon
Patent: US2007/112019 A1, 2007 ;
Location in patent: Page/Page column 9/1 ;
反应条件
potassium permanganate; water; potassium carbonate
参考文献
Journal of the Chemical Society, , p. 3061,3065
反应条件
1: With sulfuric acid in water
T=90°C; 2 h;
2: With water; sodium nitrite
T=0 - 20°C; 0.0833333 h;
3: With sulfuric acid in water
T=90°C; 2.33333 h;
参考文献
N.V. ORGANON
Patent: WO2007/39563 A1, 2007 ;
Location in patent: Page/Page column 17 ;
WO 2007/039563 A1
反应条件
potassium permanganate; potassium carbonate
参考文献
Adams; Slack
Journal of the Chemical Society, 1959 , p. 3061,3065