1,4-二乙酰氨基-2-硝基苯合成路线 （共 14 条）
反应条件
ethanol; platinum Hydrogenation;
参考文献
Tanaka, Kenjiro; Shimazaki, Michiko; Murakami, Yasuoki
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 8 p. 2714 - 2722
参考文献
Buelow; Mann
Chemische Berichte, 1897 , vol. 30, p. 986
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Ladenburg
Chemische Berichte, 1884 , vol. 17, p. 148
反应条件
bei 15 Minuten langem Kochen;
参考文献
Buelow; Mann
Chemische Berichte, 1897 , vol. 30, p. 986
反应条件
ammonia T=10 - 15°C; durch Stehenlassen;
参考文献
Kleemann
Chemische Berichte, 1886 , vol. 19, p. 336
参考文献
Ladenburg
Chemische Berichte, 1884 , vol. 17, p. 148
参考文献
Buelow; Mann
Chemische Berichte, 1897 , vol. 30, p. 986
反应条件
hydrogenchloride; tin(ll) chloride
参考文献
Nietzki
Patent: DE100880 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 5, p. 556
反应条件
nitric acid; acetic acid
T=35 - 40°C; 3 h;
参考文献
Stepanova, O. P.; Golod, E. L.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 11 p. 2142 - 2145
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 11 p. 2397 - 2401
反应条件
1: acetic acid / 0.25 h / Heating
2: acetic acid / 0.25 h / Heating
3: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min
View Scheme
参考文献
Monge, Antonio; Palop, Juan A.; Cerain, Adela Lopez de; Senador, Virginia; Martinez-Crespo, Francisko J.; et al.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 10 p. 1786 - 1792
反应条件
1: acetic acid / 0.25 h / Heating
2: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min
View Scheme
参考文献
Monge, Antonio; Palop, Juan A.; Cerain, Adela Lopez de; Senador, Virginia; Martinez-Crespo, Francisko J.; et al.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 10 p. 1786 - 1792
