1,2-二甲基丙基乙酸酯合成路线 (共 14 条)
参考文献
Bailey; King
Journal of the American Chemical Society, 1955 , vol. 77, p. 75
参考文献
Froemsdorf et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 643,646
参考文献
Froemsdorf et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 643,646
反应条件
phosphate buffer; immobilized lipase PS in methanol T=30°C; pH=7.0;
参考文献
Kato, Katsuya; Irimescu, Roxana; Saito, Takao; Yokogawa, Yoshiyuki; Takahashi, Haruo
Bioscience, Biotechnology and Biochemistry, 2003 , vol. 67, # 1 p. 203 - 206
反应条件
4-(N,N-dimethlyamino)pyridine; potassium carbonate in ethyl acetate
T=20°C; 24 h;
参考文献
Hatzakis, Nikos S.; Smonou, Ioulia
Bioorganic Chemistry, 2005 , vol. 33, # 4 p. 325 - 337
反应条件
1: acetic acid With 9-mesityl-10-methylacridinium tetrafluoroborate; sodium acetate; thiophenol in 1,2-dichloro-ethane
T=0 - 23°C; 0.25 h; Inert atmosphere;
2: 2-methyl-but-2-ene in 1,2-dichloro-ethane
96 h; Inert atmosphereIrradiation; regioselective reaction;
参考文献
Perkowski, Andrew J.; Nicewicz, David A.
Journal of the American Chemical Society, 2013 , vol. 135, # 28 p. 10334 - 10337
反应条件
dihydrogen peroxide in water; acetonitrile
T=75°C; Baeyer-Villiger oxidation; 12 h;
参考文献
Yang, Zhi-Wang; Niu, Leng-Yuan; Jia, Xiao-Jie; Kang, Qiao-Xiang; Ma, Zhen-Hong; Lei, Zi-Qiang
Catalysis Communications, 2011 , vol. 12, # 9 p. 798 - 802
反应条件
pyridine; diethyl ether
参考文献
Sarel; Newman
Journal of the American Chemical Society, 1956 , vol. 78, p. 5416,5418
反应条件
sodium tetrahydroborate in dichloromethane; water
T=20°C; 0.5 h;
参考文献
Giese, Bernd; Erfort, Ulrich
Chemische Berichte, 1983 , vol. 116, # 3 p. 1240 - 1251
反应条件
T=150°C; Yield given. Yields of byproduct given;
参考文献
Katritzky, Alan R.; Dega-Szafran, Zofia; Lopez-Rodriguez, Maria L.; King, Roy W.
Journal of the American Chemical Society, 1984 , vol. 106, # 19 p. 5577 - 5585