2,2,4-三甲基-4-硝基戊烷合成路线 （共 13 条）
反应条件
(i) Na2S, sulfur, DMSO, (ii) Al-Hg, H2O, THF; Multistep reaction;
参考文献
Kornblum,N.; Widmer,J.
Journal of the American Chemical Society, 1978 , vol. 100, p. 7086 - 7088
反应条件
azodibutyronitrile; tri-n-butyl-tin hydride in benzene 2 h; Heating;
参考文献
Ono, Noboru; Miyake, Hideyoshi; Kamimura, Akio; Hamamoto, Isami; Tamura, Rui; Kaji, Aritsune
Tetrahedron, 1985 , vol. 41, # 19 p. 4013 - 4024
反应条件
in 1,3,5-trimethyl-benzene T=200°C; 14 h;
参考文献
Tetrahedron Letters, , vol. 29, # 23 p. 2805 - 2808
反应条件
nickel Hydrogenation;
参考文献
Nametkin; Sabrodina
Doklady Akademii Nauk SSSR, 1951 , vol. 81, p. 55
Chem.Abstr., 1952 , p. 6077
反应条件
in 1,3,5-trimethyl-benzene T=200°C; 14 h;
参考文献
Tetrahedron Letters, , vol. 29, # 23 p. 2805 - 2808
反应条件
ozone in dichloromethane
T=-78°C;
参考文献
Corey, E. J.; Samuelsson, Bertil; Luzzio, Frederick A.
Journal of the American Chemical Society, 1984 , vol. 106, # 12 p. 3682 - 3683
反应条件
potassium permanganate; magnesium sulfate; acetone
参考文献
Kornblum et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 4003
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Kornblum; Jones
Organic Syntheses, 1963 , vol. 43, p. 87,89
反应条件
in dimethyl sulfoxide
T=75°C; 48 h;
参考文献
Katritzky, Alan R.; Kashmiri, M. Akram; Wittmann, Dieter K.
Tetrahedron, 1984 , vol. 40, # 9 p. 1501 - 1510
反应条件
sodium hydride
1.) CH3OH, 2.) DMSO, 80 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Katritzky, Alan R.; Kashmiri, M. Akram; Ville, George Z. de; Patel, Ranjan C.
Journal of the American Chemical Society, 1983 , vol. 105, # 1 p. 90 - 96
反应条件
water; nitric acid
T=145°C;
参考文献
Nametkin; Sabrodina
Doklady Akademii Nauk SSSR, 1950 , vol. 75, p. 395,543, 701
Chem.Abstr., 1951 , p. 6998,6999,7519
