4,4'-二甲氧基二苯二硫合成路线 (共 122 条)
反应条件
potassium carbonate in acetonitrile T=100°C; 0.5 h; Microwave irradiation;
参考文献
Chemical Communications, , # 11 p. 1410 - 1412
反应条件
silica gel 6.5 h; Mechanism; regioselective reaction;
参考文献
Kundu, Samir; Roy, Babli; Basu, Basudeb
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 26 - 33
反应条件
TPP; oxygen in ethanol; tert-butyl alcohol T=15°C; 0.1 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 22, # 30 p. 2919 - 2922
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile 2 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 68, # 6 p. 1655 - 1660
反应条件
sodium tetrahydroborate in tetrahydrofuran T=0°C; 1 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 35, # 5 p. 1770 - 1776
反应条件
disulfur dichloride; Kaolinitic clay in dichloromethane 2 h; Ambient temperature;
参考文献
Chemistry Letters, , # 1 p. 43 - 44
反应条件
1.1: 80 percent / H2 / palladium on charcoal / ethanol / 24 h / 20 °C / 3102.89 Torr 2.1: sodium nitrite / acetic acid; H2O / 0.25 h / 0 °C 2.2: 90 percent / sodium azide / acetic acid; H2O / 0 °C 3.1: 18 percent / 10 h / Heating View Scheme
参考文献
Heterocycles, , vol. 51, # 9 p. 2103 - 2109
反应条件
zinc in benzene T=6 - 8°C;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 35, p. 375 - 386
反应条件
sulfur; copper(l) iodide; lithium hydroxide hydrate in N,N-dimethyl-formamide T=100°C; 168 h; Inert atmosphere;
参考文献
Organometallics, , vol. 32, # 19 p. 5514 - 5522
反应条件
tert.-butylnitrite; C29H23N6Ru2(2+)*2Cl(1-)*6H2O; toluene-4-sulfonic acid in acetonitrile T=25°C; 1 h; Reagent/catalyst;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 30 p. 7860 - 7864
Angew. Chem., , vol. 125, # 30 p. 8014 - 8018,5