3-(苄基硫代)丙酸甲酯合成路线 (共 14 条)
参考文献
Sperna Weiland,J.H.
Recueil des Travaux Chimiques des Pays-Bas, 1964 , vol. 83, p. 81 - 93
反应条件
1: benzyl chloride With choline chloride urea; thiourea
T=60°C; Green chemistry;
2: acrylic acid methyl ester With sodium hydroxide in water
1.33333 h; HeatingGreen chemistry; TemperatureReagent/catalyst;
参考文献
Azizi, Najmedin; Yadollahy, Zahra; Rahimzadeh-Oskooee, Amin
Tetrahedron Letters, 2014 , vol. 55, # 10 p. 1722 - 1725
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile
T=20°C; 4 h;
参考文献
Yeom, Chang-Eun; Kim, Mi Jeong; Kim, B. Moon
Tetrahedron, 2007 , vol. 63, # 4 p. 904 - 909
反应条件
sodium hydroxide in water
T=20°C; Michael addition; 0.25 h;
参考文献
Zhao, Yan; Ge, Ze-Mei; Cheng, Tie-Ming; Li, Run-Tao
Synlett, 2007 , # 10 p. 1529 - 1532
反应条件
triethylamine in ethanol; water
T=30°C; 6 h; Green chemistry; Reagent/catalystSolventTemperature;
参考文献
Gao, Pengchao; Leng, Penglin; Sun, Qi; Wang, Xin; Ge, Zemei; Li, Runtao
RSC Advances, 2013 , vol. 3, # 38 p. 17150 - 17155
反应条件
triethylamine in ethanol; water
T=30°C; 6 h; Green chemistry;
参考文献
Gao, Pengchao; Leng, Penglin; Sun, Qi; Wang, Xin; Ge, Zemei; Li, Runtao
RSC Advances, 2013 , vol. 3, # 38 p. 17150 - 17155
反应条件
1: With indium; chloro-trimethyl-silane in acetonitrile
Michael addition; 5.5 h; sonication;
2: With water in acetonitrile
Further stages.;
参考文献
Ranu, Brindaban C.; Mandal, Tanmay
Synthetic Communications, 2007 , vol. 37, # 9 p. 1517 - 1523
反应条件
Helminthosporium species NRRL 4671; calcium carbonate
1.) EtOH, 27 deg C, 48 h; Yield given. Multistep reaction;
参考文献
Holland, Herbert L.; Brown, Frances M.; Lakshmaiah, Gingipalli; Larsen, Brett G.; Patel, Manish
Tetrahedron Asymmetry, 1997 , vol. 8, # 5 p. 683 - 697
反应条件
Helminthosporium species NRRL 4671; calcium carbonate
1.) EtOH, 27 deg C, 48 h; Yield given. Multistep reaction;
参考文献
Holland, Herbert L.; Brown, Frances M.; Lakshmaiah, Gingipalli; Larsen, Brett G.; Patel, Manish
Tetrahedron Asymmetry, 1997 , vol. 8, # 5 p. 683 - 697
参考文献
Andersson, Malin A.; Allenmark, Stig G.
Tetrahedron, 1998 , vol. 54, # 50 p. 15293 - 15304