1: potassium periodate, aq. H2SO4 / methanol / 0.17 h / 40 °C 2: 4.6 g 3: tetrahydrofuran; dimethylsulfoxide / 10 h / Ambient temperature 4: 0.28 g / LiAlH4 / tetrahydrofuran / 24 h / Ambient temperature View Scheme
参考文献
Majee
Journal of the Indian Chemical Society, 2012 , vol. 89, # 10 p. 1435 - 1438
1: 0.56 g / phosphonium iodide, AcOH 2: 0.51 g / pyridine / 15 h / -5 °C 3: 0.30 g / NaI / acetone / 16 h / Heating 4: 0.26 g / NaBH4 / dimethylformamide / 1 h / 80 °C View Scheme
参考文献
Majee, R. N.; Ramani, R.
Journal of the Indian Chemical Society, 1993 , vol. 70, # 2 p. 167 - 168