2-乙酰氨基-6-甲基嘧啶合成路线 （共 34 条）
参考文献
Journal of Organic Chemistry, , vol. 61, # 14 p. 4623 - 4633
反应条件
1: T=70°C; 1.5 h; 2: With sodium hydrogencarbonate in water pH=8;
参考文献
WO2006/21448 A1, ;
Page/Page column 51-52 ;
反应条件
triethylamine in dichloromethane T=5 - 20°C;
参考文献
Journal of Physical Chemistry A, , vol. 114, # 38 p. 10421 - 10426
反应条件
in dichloromethane; acetic anhydride
反应条件
sodium tris(acetoxy)borohydride T=-40 - 0°C; 7 h;
参考文献
Tetrahedron Letters, , vol. 46, # 26 p. 4487 - 4490
反应条件
acetyl chloride T=100 - 130°C; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 58, # 4 p. 887 - 891
反应条件
1: 84 percent / aq. hydroxylammonium sulfate, aq. NaOH / 2 h / Ambient temperature 2: 69 percent Chromat. / acetyl chloride (AcCl) / 4 h / 100 - 130 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 4 p. 887 - 891
反应条件
1: petroleum; sodium amide / 125 - 130 °C 2: benzene View Scheme
参考文献
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 50, p. 536
Chem. Zentralbl., , vol. 94, # III p. 1022
反应条件
acetyl chloride T=100 - 130°C; 6 h; var. cyclization / acetylating agents; influence of HCl; influence of pyridine; var. reaction times; other reaction temperature; other 5-oximinoalkanenitriles; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 58, # 4 p. 887 - 891
参考文献
U.S. Dep. Agric. ARS, 33 - 14 <1955> 4
