二((1,1'-联苯)-4-基)二氮烯合成路线 (共 36 条)
反应条件
ammonium formate; nickel in methanol T=20°C; 0.3 h;
参考文献
Srinivasa; Abiraj; Gowda, D. Channe
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 1 p. 192 - 195
反应条件
T=40°C; Zersetzung des Reaktionsprodukts mit Eis und Salzsaeure;
参考文献
Pummerer; Binapfl
Chemische Berichte, 1921 , vol. 54, p. 2771
反应条件
1: tin dichloride; hydrochloric acid; alcohol 2: Diazotization.Verkochen der Diazoniumverbindung mit Wasser View Scheme
参考文献
Friebel; Rassow
Journal fuer Praktische Chemie (Leipzig), 1901 , vol. <2> 63, p. 459
反应条件
lead; triethylammonium formate in methanol
T=20°C; 2.5 h;
参考文献
Srinivasa; Abiraj; Gowda, D. Channe
Tetrahedron Letters, 2003 , vol. 44, # 31 p. 5835 - 5837
反应条件
silver
T=200°C; P=0.0750075 Torr; 6 h;
参考文献
Boz, Serpil; Stoehr, Meike; Soydaner, Umut; Mayor, Marcel
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 3179 - 3183
Angewandte Chemie, 2009 , vol. 121, p. 3225 - 3229
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethanol; water; toluene
16 h; Inert atmosphereReflux;
参考文献
Boz, Serpil; Stoehr, Meike; Soydaner, Umut; Mayor, Marcel
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 3179 - 3183
Angewandte Chemie, 2009 , vol. 121, p. 3225 - 3229
反应条件
sodium ditelluride in tetrahydrofuran; N,N-dimethyl-formamide
T=70°C; 5 h;
参考文献
Suzuki, Hitomi; Manabe, Hajime; Kawaguchi, Takashi; Inouye, Masahiko
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 771 - 772
反应条件
Ru/C; sodium hydroxide in tetrahydrofuran; ethanol
T=105°C; 24 h; Microwave irradiation;
参考文献
Kim, Ju Hyun; Park, Ji Hoon; Chung, Young Keun; Park, Kang Hyun
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 13 p. 2412 - 2418
反应条件
T=-196.15 - 19.85°C; Elimination; dimerization; 48 h; Photolysis;
参考文献
Sasaki, Akito; Mahe, Loic; Izuoka, Akira; Sugawara, Tadashi
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 6 p. 1259 - 1275
反应条件
palladium 10 on activated carbon; hydrogen; cyclohexanecarbaldehyde in ethanol; water
P=760.051 Torr; 22 h; Reflux;
参考文献
Lunde, Sindre A.; Sydnes, Magne O.
Synlett, 2013 , vol. 24, # 18 art. no. ST-2013-P0697-SP, p. 2340 - 2344